Compact Process for the Preparation of Microfine · The procedure was performed for 30 min in a vibration ball milling machine with the frequency of 1400 Hz The milling is in argon atmosphere with a ball to powder ratio of 10 1 To avoid the overheating of milling cans the mill was paused for 5 min after a 5 min run and 2 wt % alcohol was added to reduce the bonding between balls and powders